3SOX
Structure of UHRF1 PHD finger in the free form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | OTHER |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 53.746, 53.805, 128.476 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.013 - 2.650 |
R-factor | 0.2504 |
Rwork | 0.248 |
R-free | 0.29430 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3SOU CHAIN A |
RMSD bond length | 0.012 |
RMSD bond angle | 1.700 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | PHENIX (1.6.4_486) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 30.000 | 2.740 |
High resolution limit [Å] | 2.650 | 5.700 | 2.650 |
Rmerge | 0.064 | 0.029 | 0.845 |
Number of reflections | 5681 | ||
<I/σ(I)> | 18.9 | 3.1 | |
Completeness [%] | 99.5 | 98.6 | 99.1 |
Redundancy | 7 | 6.4 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 291 | 2 M ammonium sulfate, 0.1 M Tris, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 291K |