3SIR
Crystal Structure of drICE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-04-23 |
Detector | RIGAKU JUPITER 210 |
Spacegroup name | P 31 |
Unit cell lengths | 56.025, 56.025, 287.441 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.970 - 2.680 |
R-factor | 0.1684 |
Rwork | 0.165 |
R-free | 0.23517 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1i3o |
RMSD bond length | 0.003 |
RMSD bond angle | 0.714 |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.680 |
Number of reflections | 27960 |
Completeness [%] | 98.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.4 | 291 | 0.1M Acetate pH4.4, 1.0M (NH4)2SO4, VAPOR DIFFUSION, HANGING DROP, temperature 291K |