3RYB
Lactococcal OppA complexed with SLSQSLSQS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 70 |
Detector technology | CCD |
Collection date | 2009-09-25 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.934 |
Spacegroup name | P 1 |
Unit cell lengths | 42.379, 58.921, 61.404 |
Unit cell angles | 100.66, 101.31, 103.45 |
Refinement procedure
Resolution | 30.700 - 1.500 |
R-factor | 0.1645 |
Rwork | 0.163 |
R-free | 0.20050 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3drf chain A |
RMSD bond length | 0.011 |
RMSD bond angle | 1.328 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.1.4) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.730 | 4.240 | 1.610 |
High resolution limit [Å] | 1.500 | 3.010 | 1.500 |
Rmerge | 0.034 | 0.016 | 0.281 |
Number of reflections | 83652 | 6567 | 14543 |
<I/σ(I)> | 15.78 | 41.34 | 2.9 |
Completeness [%] | 93.4 | 93.1 | 92.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 0.2M NACL, 0.1M NA-HEPES, 20% PEG 6000, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |