3RUJ
Crystal Structure of N-terminal region of yeast Atg7
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
Synchrotron site | Photon Factory |
Beamline | AR-NE3A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-10-09 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0, 0.9795, 0.9798, 0.95 |
Spacegroup name | I 41 |
Unit cell lengths | 112.846, 112.846, 102.248 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.260 - 2.100 |
R-factor | 0.2292 |
Rwork | 0.228 |
R-free | 0.25410 |
Structure solution method | MAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.319 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | PHENIX ((phenix.refine: 1.7_650)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.262 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 31750 | |
Completeness [%] | 99.2 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 295 | 0.1M Na-Hepes pH 8.0, 1.5M LiSO4H2O, 0.01M spermidine tetrahydrochloride, VAPOR DIFFUSION, HANGING DROP, temperature 295K |