Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | OTHER |
| Temperature [K] | 277 |
| Detector technology | FILM |
| Collection date | 1989-11-01 |
| Detector | CEA Reflex 25 |
| Wavelength(s) | 1.10 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 86.200, 86.200, 35.660 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 18.400 - 1.650 |
| R-factor | 0.17574 |
| Rwork | 0.175 |
| R-free | 0.19848 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 2MM1 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.995 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 18.400 |
| High resolution limit [Å] | 1.650 |
| Rmerge | 0.080 |
| Number of reflections | 17640 |
| Completeness [%] | 95.0 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 250 mM Tris-HCl, 80% Ammonium Sulfate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
