3QOB
Mechanical Coupling Controls Cooperative Ligand Binding in a Homodimeric Hemoglobin
Experimental procedure
Experimental method | LAUE |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-ID-B |
Synchrotron site | APS |
Beamline | 14-ID-B |
Temperature [K] | 288 |
Detector technology | AREA DETECTOR |
Collection date | 2008-11-06 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.017 - 1.2 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 93.250, 43.980, 83.500 |
Unit cell angles | 90.00, 122.03, 90.00 |
Refinement procedure
Resolution | 38.200 - 1.600 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 3sdh |
Refinement software | dynamiX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 38.200 |
High resolution limit [Å] | 1.600 |
Rmerge | 0.060 |
Number of reflections | 27844 |
<I/σ(I)> | 24.7 |
Completeness [%] | 74.5 |
Redundancy | 3.27 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |