3QIS
Recognition of the F&H motif by the Lowe Syndrome protein OCRL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 2009-12-12 |
Detector | RIGAKU RAXIS IV++ |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 73.478, 73.478, 145.294 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.051 - 2.300 |
R-factor | 0.1975 |
Rwork | 0.195 |
R-free | 0.23800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qv2 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.900 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.6.4_486) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 63.634 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 20465 | |
<I/σ(I)> | 15 | 2.5 |
Completeness [%] | 94.8 | 93.1 |
Redundancy | 10.6 | 10.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.3 | 291 | 1.7 M ammonium sulfate, 0.1 M MES, pH 6.3, VAPOR DIFFUSION, HANGING DROP, temperature 291K |