3QDD
HSP90A N-terminal domain in complex with BIIB021
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-E DW |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2008-05-20 |
| Detector | RIGAKU RAXIS IV++ |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 66.625, 91.064, 99.205 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 49.629 - 1.790 |
| R-factor | 0.17349 |
| Rwork | 0.172 |
| R-free | 0.20938 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.570 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.629 | 1.850 |
| High resolution limit [Å] | 1.790 | 1.790 |
| Rmerge | 0.052 | 0.454 |
| Number of reflections | 28291 | |
| Completeness [%] | 99.0 | 97.4 |
| Redundancy | 4.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 277 | 0.1 M sodium cacodylate, 20% PEG2000 MME, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
