3Q6V
Crystal Structure of Serratia fonticola Sfh-I: glycerol complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-08-08 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9795 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 32.830, 87.280, 72.570 |
Unit cell angles | 90.00, 90.85, 90.00 |
Refinement procedure
Resolution | 26.230 - 1.370 |
R-factor | 0.1644 |
Rwork | 0.163 |
R-free | 0.19560 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.322 |
Data scaling software | SCALA (3.3.9) |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.562 | 1.450 |
High resolution limit [Å] | 1.370 | 1.370 |
Rmerge | 0.056 | 0.550 |
Number of reflections | 84788 | |
<I/σ(I)> | 3.3 | |
Completeness [%] | 99.8 | 100 |
Redundancy | 7.1 | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 0.2M sodium acetate, 27% w/v PEG 3350, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |