3Q0Y
N-terminal domain of C. reinhardtii SAS-6 homolog Bld12p
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-09-14 |
Detector | MAR225 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 87.650, 95.430, 92.010 |
Unit cell angles | 90.00, 111.65, 90.00 |
Refinement procedure
Resolution | 19.918 - 2.100 |
R-factor | 0.183 |
Rwork | 0.181 |
R-free | 0.21830 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.028 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX (1.6.1_357) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 95.550 | 2.200 | |
High resolution limit [Å] | 2.100 | 4.000 | 2.100 |
Rmerge | 0.109 | 0.037 | 0.589 |
Number of reflections | 82040 | 11930 | 10636 |
<I/σ(I)> | 11.62 | 31.7 | 2.6 |
Completeness [%] | 99.7 | 98.8 | 99.8 |
Redundancy | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 298 | 20% PEG 4000, 100 MM HEPES, PH 7.0, VAPOR DIFFUSION, temperature 298K |