3P6Y
CF Im25-CF Im68-UGUAA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 104.783, 129.419, 111.159 |
Unit cell angles | 90.00, 94.01, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.900 |
R-factor | 0.22877 |
Rwork | 0.226 |
R-free | 0.27548 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3p5t |
RMSD bond length | 0.006 |
RMSD bond angle | 1.005 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASES |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.978 |
High resolution limit [Å] | 2.900 | 2.900 |
Number of reflections | 59607 | |
Completeness [%] | 95.9 | 95.92 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 283 | 15% PEG 3350, 9% dioxane and 0.1M sodium citrate, pH 5.0, VAPOR DIFFUSION, SITTING DROP, temperature 283K |