3P46
Integrin binding collagen peptide
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2008-03-13 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.5418 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 84.018, 17.288, 26.048 |
| Unit cell angles | 90.00, 91.35, 90.00 |
Refinement procedure
| Resolution | 22.370 - 1.700 |
| R-factor | 0.19837 |
| Rwork | 0.196 |
| R-free | 0.24016 |
| RMSD bond length | 0.028 |
| RMSD bond angle | 2.816 |
| Data reduction software | CrystalClear |
| Data scaling software | CrystalClear |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 22.370 |
| High resolution limit [Å] | 1.700 |
| Rmerge | 0.052 |
| Number of reflections | 4110 |
| <I/σ(I)> | 14.1 |
| Completeness [%] | 94.8 |
| Redundancy | 3.45 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 277 | 2.0 M ammonium sulfate, 50 mM Tris pH 7.5, 0.1 M Lithium sulfate, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
