3O03
Quaternary complex structure of gluconate 5-dehydrogenase from streptococcus suis type 2
Replaces: 3CXTExperimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU RAXIS IV |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 71.244, 75.272, 98.700 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 25.870 - 1.900 |
| R-factor | 0.194 |
| Rwork | 0.191 |
| R-free | 0.24200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3cxr |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.637 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 59.870 | 25.870 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.068 | |
| Number of reflections | 24607 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
