3NE3
Mycobacterium tuberculosis Acyl Carrier Protein Synthase Apo structure
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 14-ID-B |
| Synchrotron site | APS |
| Beamline | 14-ID-B |
| Temperature [K] | 120 |
| Detector technology | CCD |
| Collection date | 2000-01-01 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.97 |
| Spacegroup name | H 3 |
| Unit cell lengths | 67.933, 67.933, 83.982 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 48.190 - 1.900 |
| R-factor | 0.249 |
| Rwork | 0.248 |
| R-free | 0.27400 |
| RMSD bond length | 0.036 |
| RMSD bond angle | 2.649 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | CNS |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 48.190 |
| High resolution limit [Å] | 1.900 |
| Rmerge | 0.030 |
| Number of reflections | 10843 |
| <I/σ(I)> | 54 |
| Completeness [%] | 100.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 5.6% PEG 4K, 0.07 M sodium acetate pH 4.6 to 5.5, 30% glycerol, EVAPORATION |
