3LYN
STRUCTURE OF GREEN ABALONE LYSIN DIMER
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL9-1 |
| Synchrotron site | SSRL |
| Beamline | BL9-1 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1998-05-01 |
| Detector | MARRESEARCH |
| Spacegroup name | P 61 |
| Unit cell lengths | 119.170, 119.170, 51.290 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 100.000 - 1.700 |
| R-factor | 0.215 * |
| R-free | 0.25900 * |
| Structure solution method | MIR |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.890 * |
| Data reduction software | MOSFLM |
| Data scaling software | CCP4 ((SCALA)) |
| Phasing software | SOLVE |
| Refinement software | SHELXL |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 25.700 | 1.750 |
| High resolution limit [Å] | 1.710 | 1.710 |
| Rmerge | 0.051 * | 0.387 * |
| Number of reflections | 44479 | |
| <I/σ(I)> | 9.7 | 1.9 |
| Completeness [%] | 97.8 | 92.1 |
| Redundancy | 4.4 | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4 | 1.26 M AMMONIUM SULFATE 0.10 M SODIUM ACETATE 0.20 M SODIUM CHLORIDE, pH 4.0 |
