3LY5
DDX18 dead-domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-09-24 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97890 |
Spacegroup name | P 31 |
Unit cell lengths | 41.340, 41.340, 230.541 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.420 - 2.800 |
R-factor | 0.247 |
Rwork | 0.246 |
R-free | 0.27400 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.952 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.15) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 76.847 |
High resolution limit [Å] | 2.700 |
Number of reflections | 12190 |
Completeness [%] | 100.0 |
Redundancy | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.6 | 293 | 0.1 M HEPES pH 6.6, 0.2 M sodium thiocyanate, 20% w/v PEG 3350, VAPOR DIFFUSION, SITTING DROP, temperature 293K |