Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-05-15 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 1.0000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 70.530, 61.890, 70.140 |
| Unit cell angles | 90.00, 112.54, 90.00 |
Refinement procedure
| Resolution | 42.520 - 1.340 |
| R-factor | 0.1274 |
| Rwork | 0.127 |
| R-free | 0.14271 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.332 |
| Refinement software | REFMAC (5.6.0041) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 42.520 | 1.360 |
| High resolution limit [Å] | 1.340 | 1.340 |
| Number of reflections | 119377 | |
| <I/σ(I)> | 11.9 | 2.4 |
| Completeness [%] | 99.7 | 90.3 |
| Redundancy | 3.6 | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 300 | 0.1M Tris-HCl pH 8.0, 1.8M (NH4)2SO4, VAPOR DIFFUSION, SITTING DROP, temperature 300.0 K |
