3KYT

Crystal structure of orphan nuclear receptor RORgamma in complex with natural ligand

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-F
Synchrotron site	APS
Beamline	21-ID-F
Spacegroup name	P 41 21 2
Unit cell lengths	53.978, 53.978, 162.583
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.840 - 2.350
R-factor	0.20239
Rwork	0.197
R-free	0.29800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.019
RMSD bond angle	1.945
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.350
Number of reflections	10736
<I/σ(I)>	22.7
Redundancy	10.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1