3KY9
Autoinhibited Vav1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-12-15 |
Detector | SBC-3 |
Wavelength(s) | 1.28317 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 85.376, 58.738, 160.721 |
Unit cell angles | 90.00, 97.31, 90.00 |
Refinement procedure
Resolution | 47.286 - 2.731 |
R-factor | 0.2254 |
Rwork | 0.223 |
R-free | 0.27050 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.150 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MLPHARE |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.300 | 2.780 |
High resolution limit [Å] | 2.730 | 2.730 |
Rmerge | 0.076 | 0.959 |
Number of reflections | 42421 | |
<I/σ(I)> | 44.8 | 2 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 14.3 | 12.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 298 | 0.02 M TRIS, 0.05 M NACL, 5% GLYCEROL, 2 mM TCEP, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 298K |