3KLP
17beta-HSD1 in complex with A-diol
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU RAXIS II |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 122.440, 44.020, 60.980 |
| Unit cell angles | 90.00, 99.70, 90.00 |
Refinement procedure
| Resolution | 18.650 - 2.500 |
| R-factor | 0.17276 |
| Rwork | 0.169 |
| R-free | 0.25381 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.028 |
| RMSD bond angle | 2.512 |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 18.650 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 8781 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
