3K89

Structure of X. oryzae pv. oryzae KACC10331, Xoo0880(fabD) complexed with glycerol

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 4A
Synchrotron site	PAL/PLS
Beamline	4A
Temperature [K]	100
Detector technology	CCD
Collection date	2009-07-21
Detector	ADSC QUANTUM 210
Wavelength(s)	1.00000
Spacegroup name	P 21 21 21
Unit cell lengths	41.361, 74.095, 98.617
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	25.730 - 1.600
R-factor	0.18044
Rwork	0.179
R-free	0.20974
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3EEN
RMSD bond length	0.010
RMSD bond angle	1.227
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	MOLREP
Refinement software	REFMAC (5.5.0072)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	25.730	1.640
High resolution limit [Å]	1.600	1.599
Number of reflections	38753
Completeness [%]	99.8	99.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	9	287	pH 9.0, VAPOR DIFFUSION, HANGING DROP, temperature 287K