Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL1-5 |
Synchrotron site | SSRL |
Beamline | BL1-5 |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 1997-12-05 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0688, 0.9800, 0.9795, 0.9322 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 89.943, 89.943, 46.481 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.960 - 1.900 |
R-factor | 0.204 |
Rwork | 0.202 |
R-free | 0.25900 |
Structure solution method | MAD |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | ELVES |
Refinement software | REFMAC (4) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.000 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.097 | |
Number of reflections | 23195 | |
Completeness [%] | 99.6 | 98.4 |
Redundancy | 11 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.3 | 298 | 100MM BIS-TRIS buffer only, pH 7.3, VAPOR DIFFUSION, SITTING DROP, temperature 298K |