3K07
Crystal structure of CusA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-07-30 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9795 |
Spacegroup name | H 3 2 |
Unit cell lengths | 178.393, 178.393, 285.761 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.285 - 3.521 |
R-factor | 0.239 |
Rwork | 0.237 |
R-free | 0.27900 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.874 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 3.650 |
High resolution limit [Å] | 3.520 | 3.520 |
Rmerge | 0.057 | 0.489 |
Number of reflections | 21591 | |
<I/σ(I)> | 12.2 | |
Completeness [%] | 98.5 | 100 |
Redundancy | 6.9 | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 10% PEG 3350, 0.1M Na citrate, 0.5M (NH4)2SO4, 10% Glycerol, 1% JM600 pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |