3JVG

Crystal Structure of chicken CD1-1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL7-1
Synchrotron site	SSRL
Beamline	BL7-1
Temperature [K]	100
Wavelength(s)	0.97946
Spacegroup name	P 21 21 21
Unit cell lengths	40.839, 112.124, 201.773
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	43.060 - 2.200
R-factor	0.21762
Rwork	0.216
R-free	0.25203
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3dbx
RMSD bond length	0.019
RMSD bond angle	1.913
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	REFMAC (5.5.0088)

Data quality characteristics

	Overall
Low resolution limit [Å]	43.100
High resolution limit [Å]	2.200
Number of reflections	47868
Redundancy	7.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.4	277	20% PEG 4000, 0.2 M NH4F, pH 7.4, VAPOR DIFFUSION, SITTING DROP, temperature 277K