3ISP
Crystal structure of ArgP from Mycobacterium tuberculosis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9798 |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 85.800, 116.740, 136.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.606 - 2.700 |
R-factor | 0.212 |
Rwork | 0.207 |
R-free | 0.27100 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.110 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.063 | 0.602 |
<I/σ(I)> | 25.8 | 2.6 |
Completeness [%] | 98.0 | 93 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.8 | 290 | 1.6M Na2HPO4/NaH2PO4, pH5.8, VAPOR DIFFUSION, HANGING DROP, temperature 290K |