3I77
35/99/170-loops of FXa in SGT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-C |
Synchrotron site | APS |
Beamline | 14-BM-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-04-15 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9000 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 138.351, 138.351, 81.402 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.080 - 2.100 |
R-factor | 0.16429 |
Rwork | 0.163 |
R-free | 0.19490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1os8 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.431 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.5.0088) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.080 | 2.150 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.162 | 0.624 |
Number of reflections | 21801 | |
<I/σ(I)> | 14.4 | 3.8 |
Completeness [%] | 98.9 | |
Redundancy | 10.2 | 10.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 1.5 M Ammonium sulfate, 10 mM Calcium acetate, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |