3I70

Long-wavelength structure of NtA

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Detector technology	CCD
Collection date	2009-03-15
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	1.6995
Spacegroup name	C 1 2 1
Unit cell lengths	80.229, 50.710, 54.187
Unit cell angles	90.00, 117.09, 90.00

Refinement procedure

Resolution	27.960 - 2.300
R-factor	0.221
Rwork	0.221
R-free	0.27600
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1pxu
RMSD bond length	0.006
RMSD bond angle	1.300
Refinement software	CNS (1.2)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	28.060
High resolution limit [Å]	2.300	2.300
Number of reflections	8736

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION			VAPOR DIFFUSION