3HW2
Crystal structure of the SifA-SKIP(PH) complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-10-06 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.939 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 91.799, 110.866, 44.274 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 3.300 |
R-factor | 0.2473 |
Rwork | 0.240 |
R-free | 0.30925 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3cxb |
RMSD bond length | 0.009 |
RMSD bond angle | 1.338 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0088) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 3.400 |
High resolution limit [Å] | 3.300 | 3.300 |
Total number of observations | 31607 | |
Number of reflections | 7176 | |
<I/σ(I)> | 8.9 | 3 |
Completeness [%] | 99.3 | 95.8 |
Redundancy | 4.4 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 30% PEG 4000, 0.2M Na acetate trihydrate, 0.1 M Tris-HCl, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K |