3HNZ
Structure of E. coli FabF(C163A) in Complex with Platensimycin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-07-14 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.00 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 74.665, 74.665, 146.274 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.930 - 2.750 |
R-factor | 0.182 |
Rwork | 0.178 |
R-free | 0.25600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.431 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | TNT |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 38.930 | 50.000 | 2.850 |
High resolution limit [Å] | 2.750 | 5.920 | 2.750 |
Rmerge | 0.069 | 0.028 | 0.419 |
Number of reflections | 12790 | ||
<I/σ(I)> | 18.917 | ||
Completeness [%] | 99.8 | 98.5 | 100 |
Redundancy | 3.5 | 3.2 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |