3HE4
Heterospecific coiled-coil pair SYNZIP5:SYNZIP6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-06-24 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97927 |
Spacegroup name | P 63 |
Unit cell lengths | 82.678, 82.678, 150.545 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.090 - 2.460 |
R-factor | 0.216 |
Rwork | 0.212 |
R-free | 0.25800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.681 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.090 | 2.550 |
High resolution limit [Å] | 2.460 | 2.460 |
Number of reflections | 21204 | |
<I/σ(I)> | 26.346 | |
Completeness [%] | 99.7 | 99.3 |
Redundancy | 5.8 | 5.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.2 | 295 | 100 mM TRIS, 20% MPD, pH 8.2, VAPOR DIFFUSION, HANGING DROP, temperature 295K |