3GXT

Crystal structure of alpha-galactosidase A at pH 4.5 complexed with 1-deoxygalactonijirimycin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 23-ID-D
Synchrotron site	APS
Beamline	23-ID-D
Spacegroup name	P 32 2 1
Unit cell lengths	89.610, 89.610, 216.640
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.900 - 2.700
R-factor	0.24509
Rwork	0.242
R-free	0.30577
RMSD bond length	0.017
RMSD bond angle	1.950
Data scaling software	SCALA
Refinement software	REFMAC

Data quality characteristics

	Overall
Low resolution limit [Å]	77.600
High resolution limit [Å]	2.700
Number of reflections	27633

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION			vapor diffusion