3GXM

Crystal structure of acid-beta-glucosidase at pH 4.5, phosphate crystallization condition

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 14-BM-C
Synchrotron site	APS
Beamline	14-BM-C
Spacegroup name	P 1 21 1
Unit cell lengths	110.505, 91.779, 152.751
Unit cell angles	90.00, 111.24, 90.00

Refinement procedure

Resolution	34.340 - 2.200
R-factor	0.223
Rwork	0.220
R-free	0.27600
RMSD bond length	0.016
RMSD bond angle	1.682
Refinement software	REFMAC

Data quality characteristics

	Overall
Low resolution limit [Å]	34.340
High resolution limit [Å]	2.200
Number of reflections	138784

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION			vapor diffusion