3GW0
UROD mutant G318R
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2008-08-18 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 103.266, 103.266, 73.389 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 30.700 - 2.000 |
| R-factor | 0.196 |
| Rwork | 0.194 |
| R-free | 0.24000 |
| RMSD bond length | 0.026 |
| RMSD bond angle | 1.977 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 40.000 | 40.000 | 2.070 |
| High resolution limit [Å] | 2.000 | 4.310 | 2.000 |
| Rmerge | 0.084 | 0.053 | 0.585 |
| Number of reflections | 31077 | ||
| <I/σ(I)> | 15.195 | ||
| Completeness [%] | 100.0 | 99.8 | 100 |
| Redundancy | 5.9 | 5.7 | 5.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | hanging drop | hanging drop |
