3GJP
Crystal structure of mutant coiled coil GCN4 leucine zipper
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2007-09-27 |
| Detector | RIGAKU RAXIS IV++ |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 42.246, 45.936, 47.156 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 32.900 - 2.000 |
| R-factor | 0.215 |
| Rwork | 0.212 |
| R-free | 0.26900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2o7h |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.090 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.000 | 2.150 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 6442 | |
| <I/σ(I)> | 15.7 | 7.6 |
| Completeness [%] | 98.1 | 98.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
