3FRC
Tetramerization and Cooperativity in Plasmodium falciparum glutathione transferase are mediated by the atypic loop 113-118
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X13 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X13 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MAR CCD 165 mm |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 57.472, 69.407, 123.323 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.710 - 2.000 |
| R-factor | 0.22233 |
| Rwork | 0.220 |
| R-free | 0.26784 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1q4j |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.131 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 34227 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
