3FJD
Crystal structure of L44F/F132W mutant of Human acidic fibroblast growth factor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 103 |
Detector technology | IMAGE PLATE |
Collection date | 2007-10-26 |
Detector | RIGAKU RAXIS IIC |
Wavelength(s) | 1.5418 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 73.236, 97.581, 108.451 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.070 - 1.900 |
R-factor | 0.19 |
Rwork | 0.190 |
R-free | 0.22100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jqz |
RMSD bond length | 0.009 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.070 | 1.940 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.073 | 0.350 |
Number of reflections | 28392 | |
<I/σ(I)> | 3.81 | |
Completeness [%] | 92.2 | 91.9 |
Redundancy | 12.9 | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 3.0M Na-formate, 0.2M (NH4)2SO4, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |