3FFM

The crystal structure of human Gadd45g

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE BL-5A
Synchrotron site	Photon Factory
Beamline	BL-5A
Detector technology	CCD
Collection date	2007-11-01
Detector	ADSC QUANTUM 315
Wavelength(s)	1.0000
Spacegroup name	I 21 3
Unit cell lengths	126.413, 126.413, 126.413
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.980 - 2.300
Rwork	0.233
R-free	0.25980
Structure solution method	SAD
RMSD bond length	0.006
RMSD bond angle	1.122
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SHELXS
Refinement software	CNS (1.1)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.300
Number of reflections	13290
Redundancy	10.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	298	25% PEG 3350, 0.2M Nacl, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K
2