3FCV
Crystal structure of the Mimivirus NDK +Kpn-N62L-R107G triple mutant complexed with dUDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | OXFORD DIFFRACTION ENHANCE ULTRA |
Temperature [K] | 105 |
Detector technology | CCD |
Collection date | 2007-10-07 |
Detector | OXFORD ONYX CCD |
Wavelength(s) | 1.54 |
Spacegroup name | P 63 |
Unit cell lengths | 70.407, 70.407, 104.846 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.225 - 2.400 |
R-factor | 0.192 |
Rwork | 0.189 |
R-free | 0.24700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b8p |
RMSD bond length | 0.002 |
RMSD bond angle | 0.727 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.500 | 2.530 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 9483 | |
<I/σ(I)> | 4.4 | 1.9 |
Completeness [%] | 81.8 | 81.8 |
Redundancy | 3.3 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.6 | 293 | 0.8-1.1M sodium citrate, 0.1M Tris, pH 7.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |