3F95
Crystal Structure of Extra C-terminal Domain (X) of Exo-1,3/1,4-beta-glucanase (ExoP) from Pseudoalteromonas sp. BB1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 113 |
Detector technology | IMAGE PLATE |
Collection date | 2007-07-13 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 73.416, 87.882, 56.459 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.750 - 1.800 |
R-factor | 0.19055 |
Rwork | 0.188 |
R-free | 0.23391 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.635 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 21.750 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.046 | 0.279 |
Number of reflections | 34484 | |
<I/σ(I)> | 18.5 | 3.8 |
Completeness [%] | 99.7 | 99.2 |
Redundancy | 3.3 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | 0.1M MES-NaOH, pH6.5, 25% PEG6000, 0.2M MgCl2, VAPOR DIFFUSION, HANGING DROP, temperature 291.0K |