Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE BW7A |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | BW7A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | Mar |
| Wavelength(s) | 0.96 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 79.656, 123.075, 57.239 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.700 |
| R-factor | 0.214 |
| Rwork | 0.212 |
| R-free | 0.25500 |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.745 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA (3.2.25) |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 66.872 | 37.090 | 1.790 |
| High resolution limit [Å] | 1.700 | 5.380 | 1.700 |
| Rmerge | 0.064 | 0.029 | 0.493 |
| Total number of observations | 10637 | 44437 | |
| Number of reflections | 60078 | ||
| <I/σ(I)> | 9.308 | 17.1 | 1.6 |
| Completeness [%] | 96.2 | 93.6 | 94.5 |
| Redundancy | 5.3 | 5.3 | 5.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 289 | 0.1M Tris, 0.4M sodium nitrate, 40% PEG3350, pH 7.5, vapor diffusion, hanging drop, temperature 289K |
