3F36
Apoferritin: complex with 2-isopropylphenol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-04 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 182.366, 182.366, 182.366 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.700 |
R-factor | 0.18672 |
Rwork | 0.185 |
R-free | 0.20986 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1xz1 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.367 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | REFMAC (5.4.0074) |
Refinement software | REFMAC (5.4.0074) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.540 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.057 | 0.317 |
Number of reflections | 29075 | |
<I/σ(I)> | 24.9 | 5.3 |
Completeness [%] | 99.8 | 100 |
Redundancy | 23.8 | 11.63 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | Cadmium sulfate, ammonium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 291K |