3F34
Apoferritin: complex with 2,6-diethylphenol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X6A |
Synchrotron site | NSLS |
Beamline | X6A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-07-05 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.9537 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 181.456, 181.456, 181.456 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.670 - 1.680 |
R-factor | 0.20007 |
Rwork | 0.198 |
R-free | 0.24730 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1xz1 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.392 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | REFMAC (5.4.0074) |
Refinement software | REFMAC (5.4.0074) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.080 | 1.740 |
High resolution limit [Å] | 1.680 | 1.680 |
Rmerge | 0.099 | 0.527 |
Number of reflections | 29091 | |
<I/σ(I)> | 13 | 2 |
Completeness [%] | 97.9 | 85.7 |
Redundancy | 14.83 | 5.26 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | Cadmium sulfate, ammonium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 291K |