3F33
Apoferritin: complex with propofol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-10-11 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.1 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 182.487, 182.487, 182.487 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.110 - 1.700 |
R-factor | 0.19041 |
Rwork | 0.189 |
R-free | 0.21988 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1xz1 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.230 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | REFMAC (5.4.0074) |
Refinement software | REFMAC (5.4.0074) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.250 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.070 | 0.319 |
Number of reflections | 29110 | |
<I/σ(I)> | 23.5 | 4.9 |
Completeness [%] | 99.8 | 99.9 |
Redundancy | 16.54 | 9.98 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | Cadmium sulfate, ammonium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 291K |