3F0L
Crystal structure of oxidized D105N Synechocystis sp. PcyA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL7-1 |
| Synchrotron site | SSRL |
| Beamline | BL7-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-03-31 |
| Detector | ADSC QUANTUM 315 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 70.845, 95.554, 42.690 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 39.620 - 1.300 |
| R-factor | 0.17 |
| Rwork | 0.169 |
| R-free | 0.19300 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.721 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.4.0069) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.620 | 1.330 |
| High resolution limit [Å] | 1.300 | 1.300 |
| Number of reflections | 72066 | |
| Completeness [%] | 97.6 | 95.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | 293 | 1.45M Ammonium sulfate, 0.15M NaCl, 0.1M Aacodylate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
