3EZ6

Structure of parA-ADP complex:tetragonal form

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.1
Synchrotron site	ALS
Beamline	8.2.1
Detector technology	CCD
Collection date	2007-01-02
Detector	ADSC QUANTUM 4
Wavelength(s)	1.0
Spacegroup name	P 41 21 2
Unit cell lengths	143.300, 143.300, 108.000
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	101.330 - 2.580
R-factor	0.187
Rwork	0.187
R-free	0.24000
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3ez2
RMSD bond length	0.009
RMSD bond angle	1.400
Refinement software	CNS (1.2)

Data quality characteristics

	Overall
Low resolution limit [Å]	107.800
High resolution limit [Å]	2.580
Number of reflections	35970
<I/σ(I)>	8.9
Completeness [%]	99.0
Redundancy	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	298	PEG 6000, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K