3EYM
Structure of Influenza Haemagglutinin in complex with an inhibitor of membrane fusion
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-09-09 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.97565 |
| Spacegroup name | P 41 |
| Unit cell lengths | 160.465, 160.464, 176.548 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.930 - 2.800 |
| R-factor | 0.19709 |
| Rwork | 0.197 |
| R-free | 0.21711 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.473 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 129.000 | 2.930 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Number of reflections | 103890 | |
| Completeness [%] | 99.8 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | Ammonium citratre, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
