3EVR
Crystal structure of Calcium bound monomeric GCAMP2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE A1 |
Synchrotron site | CHESS |
Beamline | A1 |
Detector technology | CCD |
Collection date | 2008-04-12 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 121.995, 121.995, 97.831 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.649 - 2.000 |
R-factor | 0.1655 |
Rwork | 0.163 |
R-free | 0.19020 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.137 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.070 |
High resolution limit [Å] | 2.000 | 4.310 | 2.000 |
Rmerge | 0.127 | 0.054 | 0.710 |
Number of reflections | 50531 | ||
<I/σ(I)> | 23.625 | ||
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 17.4 | 16.7 | 15.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |