3DXZ
Crystal structure of EcTrmB in complex with SAH
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BSRF BEAMLINE 3W1A |
| Synchrotron site | BSRF |
| Beamline | 3W1A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-06-22 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1.000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 45.570, 48.290, 57.480 |
| Unit cell angles | 90.00, 90.52, 90.00 |
Refinement procedure
| Resolution | 19.450 - 1.580 |
| R-factor | 0.17517 |
| Rwork | 0.174 |
| R-free | 0.19285 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3dxx |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.158 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 19.970 |
| High resolution limit [Å] | 1.580 |
| Number of reflections | 34161 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 283 | 15% PEG 3350 (w/v), 150 mM MgSO4, VAPOR DIFFUSION, HANGING DROP, temperature 283K |
