3DXX
Crystal structure of EcTrmB
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2007-03-18 |
| Detector | MAR scanner 345 mm plate |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 46.420, 47.010, 58.640 |
| Unit cell angles | 90.00, 90.01, 90.00 |
Refinement procedure
| Resolution | 24.790 - 2.050 |
| R-factor | 0.19457 |
| Rwork | 0.193 |
| R-free | 0.22687 |
| Structure solution method | SAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.244 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 24.790 |
| High resolution limit [Å] | 2.040 |
| Number of reflections | 15183 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 283 | 15% (w/v) PEG 3350, 150mM MgSO4, VAPOR DIFFUSION, HANGING DROP, temperature 283K |
