3DUK
CRYSTAL STRUCTURE OF A NTF2-LIKE PROTEIN OF UNKNOWN FUNCTION (MFLA_0564) FROM METHYLOBACILLUS FLAGELLATUS KT AT 2.200 A RESOLUTION
Experimental procedure
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-05-01 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.91837,0.97932,0.97911 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 103.030, 103.030, 130.950 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.981 - 2.200 |
R-factor | 0.1653 |
Rwork | 0.163 |
R-free | 0.21170 |
Structure solution method | MAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.572 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 29.981 | 29.980 | 2.280 |
High resolution limit [Å] | 2.200 | 4.720 | 2.200 |
Rmerge | 0.031 | 0.592 | |
Number of reflections | 41254 | ||
<I/σ(I)> | 12.85 | 35.4 | 2.6 |
Completeness [%] | 99.6 | 99.3 | 97.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 277 | 20.0% 2-propanol, 30.0% polyethylene glycol 4000, 0.1M citric acid pH 5.0, VAPOR DIFFUSION,SITTING DROP,NANODROP, temperature 277K, VAPOR DIFFUSION, SITTING DROP |